1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

Base Information

Chemical Name:1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide
CAS No.:80266-21-3
Molecular Formula:2BrH*C₃₀H₂₉N₅O
Molecular Weight:637.417
Hs Code.:

Synonyms:1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

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Chemical Property of 1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

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Technology Process of 1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

There total 7 articles about 1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5600-62-4
4-(4-nitrophenyl)butanoic acid

: 80266-21-3
1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

Guidance literature:: Multi-step reaction with 7 steps

1: HN₃ / CHCl₃ / 4 h / 50 °C

2: 1.) pyridine, 2.) Ac₂O / 1.) ether, 100 deg C, 0.5 h, 2.) AcOH, reflux, 1 h

3: 73 percent / H₂ / 10percent Pd/C / ethyl acetate; methanol

4: 93 percent / N-methylpyrrolidinone / benzene / 0.17 h / 50 °C

5: 73 percent / hydrazine hydrate, pyridine / 3 h / 60 °C

6: Fe, HCl

With pyridine; 1-methyl-pyrrolidin-2-one; hydrogenchloride; tris-(2-chloro-ethyl)-amine; hydrogen; acetic anhydride; iron; hydrazine hydrate; palladium on activated charcoal; In methanol; chloroform; ethyl acetate; benzene;
DOI:10.1021/jm00345a015

Reference yield:

: 80258-69-1
N-<4-(4-nitrophenyl)butyl>phthalimide

: 80266-21-3
1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / H₂ / 10percent Pd/C / ethyl acetate; methanol

2: 93 percent / N-methylpyrrolidinone / benzene / 0.17 h / 50 °C

3: 73 percent / hydrazine hydrate, pyridine / 3 h / 60 °C

4: Fe, HCl

With pyridine; 1-methyl-pyrrolidin-2-one; hydrogenchloride; hydrogen; iron; hydrazine hydrate; palladium on activated charcoal; In methanol; ethyl acetate; benzene;
DOI:10.1021/jm00345a015

Reference yield:

: 80258-63-5
4-(4-nitrophenyl)butylamine

: 80266-21-3
1-[4-(Acridin-9-ylamino)-phenyl]-3-[4-(4-amino-butyl)-phenyl]-urea; hydrobromide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) pyridine, 2.) Ac₂O / 1.) ether, 100 deg C, 0.5 h, 2.) AcOH, reflux, 1 h

2: 73 percent / H₂ / 10percent Pd/C / ethyl acetate; methanol

3: 93 percent / N-methylpyrrolidinone / benzene / 0.17 h / 50 °C

4: 73 percent / hydrazine hydrate, pyridine / 3 h / 60 °C

5: Fe, HCl

With pyridine; 1-methyl-pyrrolidin-2-one; hydrogenchloride; hydrogen; acetic anhydride; iron; hydrazine hydrate; palladium on activated charcoal; In methanol; ethyl acetate; benzene;
DOI:10.1021/jm00345a015