N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide

Base Information

Chemical Name:N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide
CAS No.:102745-77-7
Molecular Formula:C₁₄H₁₅N₃O₆
Molecular Weight:321.29
Hs Code.:
DSSTox Substance ID:DTXSID101228985

Synonyms:N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide;DTXSID101228985;102745-77-7

Suppliers and Price of N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:321.09608521
Heavy Atom Count:23
Complexity:512

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)NC1CCC(=O)C(C1)C2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide

There total 4 articles about N-[3-(2,4-Dinitrophenyl)-4-oxocyclohexyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 102745-77-7
4-acetamido-2-(2,4-dinitrophenyl)cyclohexanone

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Raney nickel / ethanol / 3 h / 180 °C / 90500.9 Torr

2: 72 percent / sodium dichromate dihydrate, conc. H₂SO₄ / H₂O / 0.33 h

3: 85 percent / toluene / 3 h / Heating

4: 2.) 3.5percent aq. HCl / 1.) CH₂Cl₂, RT, 24 h, 2.) 24 h

With hydrogenchloride; sodium dichromate; sulfuric acid; hydrogen; nickel; In ethanol; water; toluene;
DOI:10.1021/jm00158a022

Reference yield:

: 23363-88-4
trans-N-acetyl-4-hydroxycyclohexylamine

: 102745-77-7
4-acetamido-2-(2,4-dinitrophenyl)cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / sodium dichromate dihydrate, conc. H₂SO₄ / H₂O / 0.33 h

2: 85 percent / toluene / 3 h / Heating

3: 2.) 3.5percent aq. HCl / 1.) CH₂Cl₂, RT, 24 h, 2.) 24 h

With hydrogenchloride; sodium dichromate; sulfuric acid; In water; toluene;
DOI:10.1021/jm00158a022

Reference yield:

: 27514-08-5
N-(4-oxocyclohexyl)acetamide

: 102745-77-7
4-acetamido-2-(2,4-dinitrophenyl)cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / toluene / 3 h / Heating

2: 2.) 3.5percent aq. HCl / 1.) CH₂Cl₂, RT, 24 h, 2.) 24 h

With hydrogenchloride; In toluene;
DOI:10.1021/jm00158a022