C₃₀H₄₀FN₃O₈S

Base Information

Chemical Name:C₃₀H₄₀FN₃O₈S
CAS No.:1402742-33-9
Molecular Formula:C₃₀H₄₀FN₃O₈S
Molecular Weight:621.727
Hs Code.:

C<sub>30</sub>H<sub>40</sub>FN<sub>3</sub>O<sub>8</sub>S

Synonyms:C₃₀H₄₀FN₃O₈S

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Chemical Property of C₃₀H₄₀FN₃O₈S

Chemical Property:

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Technology Process of C₃₀H₄₀FN₃O₈S

There total 5 articles about C₃₀H₄₀FN₃O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402742-11-3
C₁₅H₁₃FO₂

: 1402742-33-9
C₃₀H₄₀FN₃O₈S

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: 3 h / -78 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 - 25 °C

4.1: mercaptoacetic acid; trifluoroacetic acid / 16 h / 0 - 25 °C

4.2: pH 8

5.1: acetonitrile / 16 h / 60 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 30 °C

7.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

7.2: 1 h / -78 °C

With hydrogenchloride; dmap; titanium(IV) tetraethanolate; n-butyllithium; mercaptoacetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; acetonitrile;

Reference yield:

: 1402742-12-4
C₁₉H₂₂FNO₂S

: 1402742-33-9
C₃₀H₄₀FN₃O₈S

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 3 h / -78 °C

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 - 25 °C

3.1: mercaptoacetic acid; trifluoroacetic acid / 16 h / 0 - 25 °C

3.2: pH 8

4.1: acetonitrile / 16 h / 60 °C

5.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 30 °C

6.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

6.2: 1 h / -78 °C

With hydrogenchloride; dmap; n-butyllithium; mercaptoacetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; acetonitrile;

Reference yield:

: 1402742-13-5
C₂₉H₃₇FN₂O₅S₂

: 1402742-33-9
C₃₀H₄₀FN₃O₈S

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 - 25 °C

2.1: mercaptoacetic acid; trifluoroacetic acid / 16 h / 0 - 25 °C

2.2: pH 8

3.1: acetonitrile / 16 h / 60 °C

4.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 30 °C

5.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

5.2: 1 h / -78 °C

With hydrogenchloride; dmap; n-butyllithium; mercaptoacetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; acetonitrile;