tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate

Base Information

• Chemical Name: tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate
• CAS No.: 421551-55-5
• Molecular Formula: C₃₂H₃₇N₅O₄
• Molecular Weight: 555.677

Synonyms:tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate

Chemical Property of tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate

There total 1 articles about tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 2-(((2-cyano-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate (421551-54-4) → tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate (421551-55-5)

Guidance literature:

With ammonia; hydrogen; In methanol; for 16h; under 2327.23 Torr;

DOI:10.1016/j.bmcl.2010.11.023

Reference yield:

tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate (421551-55-5) → methyl 4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-3-(aminomethyl)benzoate (422284-01-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmcl.2010.11.023

Reference yield:

tert-butyl 2-(((2-aminomethyl-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate (421551-55-5) → C31H37N5O3 (421552-23-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.bmcl.2010.11.023

upstream raw materials:

tert-butyl 2-(((2-cyano-4-(methoxycarbonyl)benzyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-1H-benzo[d]imidazole-1-carboxylate

Downstream raw materials:

C₃₁H₃₇N₅O₃

C₃₁H₃₅N₅O₄

methyl 4-((((1H-benzo[d]imidazol-2-yl)methyl)(5,6,7,8-tetrahydroquinolin-8-yl)amino)methyl)-3-(aminomethyl)benzoate

C₃₇H₄₅N₅O₆

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