N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

Base Information

Chemical Name:N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide
CAS No.:160580-60-9
Molecular Formula:C₂₃H₃₂N₂O₅Si
Molecular Weight:444.603
Hs Code.:

Synonyms:N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

Suppliers and Price of N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

Chemical Property:

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Technology Process of N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

There total 7 articles about N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 123-56-8,89963-74-6
Succinimide

: 160580-59-6
7-(tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-yn-1-ol

: 160580-60-9
N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 3h; Ambient temperature;

Reference yield:

: 10268-12-9
methyl 3-nitrophenylacetate

: 160580-60-9
N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / LDA / hexane; tetrahydrofuran / -78 °C

2: 89 percent / LiAlH₄ / tetrahydrofuran / -78 - -40 °C

3: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

4: 28 percent / LDA

5: 91 percent / DEAD, Ph₃P / tetrahydrofuran / 3 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;

Reference yield:

: 1877-73-2
3-nitro-benzeneacetic acid

: 160580-60-9
N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / H₂SO₄ / 2.5 h / Heating

2: 76 percent / LDA / hexane; tetrahydrofuran / -78 °C

3: 89 percent / LiAlH₄ / tetrahydrofuran / -78 - -40 °C

4: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

5: 28 percent / LDA

6: 91 percent / DEAD, Ph₃P / tetrahydrofuran / 3 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; sulfuric acid; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;