2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

Base Information

Chemical Name:2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide
CAS No.:1246495-07-7
Molecular Formula:C₂₀H₂₂Cl₂N₂O₃S
Molecular Weight:441.378
Hs Code.:

Synonyms:2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

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Chemical Property of 2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

Chemical Property:

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Technology Process of 2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

There total 5 articles about 2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10147-36-1
n-propanesulfonyl chloride

: C₁₇H₁₆Cl₂N₂O

: 1246495-07-7
2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: C₁₅H₂₀N₂O₃

: 1246495-07-7
2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / methanol / 2327.23 Torr

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3: hydrogenchloride / 1,4-dioxane / 20 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; hydrogen; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.01.011

Reference yield:

: C₁₅H₂₂N₂O₂

: 1246495-07-7
2,4-dichloro-N-(phenyl(1-(propylsulfonyl)azetidin-3-yl)methyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: hydrogenchloride / 1,4-dioxane / 20 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2014.01.011