dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate

Base Information

Chemical Name:dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate
CAS No.:1255460-82-2
Molecular Formula:C₁₇H₂₁NO₇
Molecular Weight:351.356
Hs Code.:

Synonyms:dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate

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Technology Process of dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate

There total 1 articles about dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 40637-56-7
dimethyl allylmalonate

: 3179-10-0
1-methoxy-4-(2-nitro-vinyl)-benzene

: 1255460-82-2
dimethyl (2R,3E,4R)-3-(hydroxyimino)-4-(hydroxymethyl)-2-(4-methoxyphenyl)cyclopentane-1,1-dicarboxylate

Guidance literature:: dimethyl allylmalonate; 1-methoxy-4-(2-nitro-vinyl)-benzene; With 9-epiquinidine; In tetrahydrofuran; at 20 ℃; for 48h;

With chloro-trimethyl-silane; triethylamine; In tetrahydrofuran; at -30 - 20 ℃;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/c0cc01940b