3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

Base Information

Chemical Name:3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole
CAS No.:1597408-85-9
Molecular Formula:C₂₈H₂₃BrN₂O₇S
Molecular Weight:611.47
Hs Code.:

Synonyms:3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

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Chemical Property of 3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

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Technology Process of 3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

There total 1 articles about 3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1597408-78-0
2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-3-methyl-9-(phenylsulfonyl)-9H-carbazole

: 1597408-85-9
3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 2h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201301524 DOI:10.1002/ejoc.201301524

Reference yield: 86.0%

: 1597408-85-9
3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

: 1597408-90-6
2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole-3-carbaldehyde

Guidance literature:: With tetra(n-butyl)ammonium dichromate(VI); In chloroform; for 10h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201301524

Reference yield:

: 1597408-85-9
3-(bromomethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-4-methoxy-9-(phenylsulfonyl)-9H-carbazole

: 1445973-99-8
2-(4,5-dimethoxy-2-nitrophenyl)-4-hydroxy-9-(phenylsulfonyl)-9H-carbazole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: tetra(n-butyl)ammonium dichromate(VI) / chloroform / 10 h / Inert atmosphere; Reflux

2: boron tribromide / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

With tetra(n-butyl)ammonium dichromate(VI); boron tribromide; In dichloromethane; chloroform;
DOI:10.1002/ejoc.201301524