(1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-ribitol

Base Information

• Chemical Name: (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-ribitol
• CAS No.: 59696-99-0
• Molecular Formula: C₁₈H₁₈N₄O₅
• Molecular Weight: 370.365

Synonyms:(1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-ribitol

Chemical Property of (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-ribitol

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-ribitol

There total 3 articles about (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O⁵-benzoyl-D-1,4-anhydro-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Hydrazino-3-nitropyridine (15367-16-5) → (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O5-benzoyl-D-1,4-anhydro-ribitol (59696-99-0)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / Pd-C / methanol

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/jo00881a012

Reference yield:

(1S)-O5-benzoyl-1-(8-nitro-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-D-1,4-anhydro-ribitol (59696-94-5) → (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O5-benzoyl-D-1,4-anhydro-ribitol (59696-99-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/jo00881a012

Reference yield:

(2Ξ)-O6-benzoyl-D-ribo-2,5-anhydro-hexonimidothioic acid benzyl ester (50908-31-1,50908-32-2,59684-39-8,68779-21-5) → (1S)-1-(8-amino-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-O5-benzoyl-D-1,4-anhydro-ribitol (59696-99-0)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / Pd-C / methanol

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/jo00881a012

upstream raw materials:

(1S)-O⁵-benzoyl-1-(8-nitro-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-D-1,4-anhydro-ribitol

(2Ξ)-O⁶-benzoyl-D-ribo-2,5-anhydro-hexonimidothioic acid benzyl ester

2-Hydrazino-3-nitropyridine

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