N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

Base Information

Chemical Name:N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide
CAS No.:1609137-66-7
Molecular Formula:C₃₃H₄₂BrNO₃
Molecular Weight:580.605
Hs Code.:

Synonyms:N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

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Chemical Property of N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

Chemical Property:

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Technology Process of N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

There total 5 articles about N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1609137-63-4
[3',5'-bis(hexyloxy)biphenyl-4-yl]methanamine

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 1609137-66-7
N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 16h;
DOI:10.1002/chem.201400323

Reference yield:

: 111-25-1
1-bromo-hexane

: 1609137-66-7
N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 12 h / Reflux

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/chem.201400323

Reference yield:

: 1609137-62-3
3',5'-bis(hexyloxy)biphenyl-4-carbonitrile

: 1609137-66-7
N-{[3',5'-bis(hexyloxy)biphenyl-4-yl]methyl}-2-(4-bromophenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201400323