C₄₇H₅₄N₆O₉

Base Information

Chemical Name:C₄₇H₅₄N₆O₉
CAS No.:1379654-53-1
Molecular Formula:C₄₇H₅₄N₆O₉
Molecular Weight:846.981
Hs Code.:

C<sub>47</sub>H<sub>54</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₄₇H₅₄N₆O₉

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Chemical Property of C₄₇H₅₄N₆O₉

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Technology Process of C₄₇H₅₄N₆O₉

There total 6 articles about C₄₇H₅₄N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₇H₅₆N₆O₁₀

: 1379654-53-1
C₄₇H₅₄N₆O₉

Guidance literature:: C₄₇H₅₆N₆O₁₀; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

In N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1002/chem.201103185

Reference yield:

: 1379654-52-0
C₅₂H₆₄N₆O₁₂

: 1379654-53-1
C₄₇H₅₄N₆O₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / chloroform / 2 h / 0 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 96 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103185

Reference yield:

: C₂₈H₃₀N₂O₅

: 1379654-53-1
C₄₇H₅₄N₆O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 48 h / 0 - 20 °C

2.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C

2.2: 22 h / 20 °C

3.1: trifluoroacetic acid / chloroform / 2 h / 0 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / N,N-dimethyl-formamide / 1 h / 0 °C

4.2: 96 h / 20 °C

With lithium hydroxide monohydrate; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103185