O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

Base Information

Chemical Name:O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate
CAS No.:1442742-97-3
Molecular Formula:C₈₁H₁₂₈O₁₆
Molecular Weight:1357.9
Hs Code.:

Synonyms:O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

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Chemical Property of O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

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Technology Process of O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

There total 9 articles about O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1158602-58-4
4-oxo-4-(prop-2-yn-1-yloxy)butanoic anhydride

: 1235584-51-6
2,2-bis(hydroxymethyl)propane-1,3-diyl bis(3,4-bis(dodecyloxy)benzoate)

: 1442742-97-3
O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 25 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ja403323y

Reference yield:

: 115-77-5
Pentaerythritol

: 1442742-97-3
O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

Guidance literature:: Multi-step reaction with 4 steps

1.1: water / 60 °C

1.2: 3 h / 25 °C

2.1: dicyclohexyl-carbodiimide; S-phenyl 4-methoxybenzenesulfinothioate / dichloromethane / 12 h / 25 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / methanol; dichloromethane / 12 h / 25 °C

4.1: dmap; pyridine / dichloromethane / 20 h / 25 °C / Inert atmosphere

With pyridine; dmap; palladium on activated charcoal; S-phenyl 4-methoxybenzenesulfinothioate; hydrogen; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1021/ja403323y

Reference yield:

: 2425-41-4
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

: 1442742-97-3
O,O'-(2,2-bis(((3,4-bis(dodecyloxy)benzoyl)oxy)methyl)propane-1,3-diyl) di(prop-2-yn-1-yl) disuccinate

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide; S-phenyl 4-methoxybenzenesulfinothioate / dichloromethane / 12 h / 25 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen / methanol; dichloromethane / 12 h / 25 °C

3: dmap; pyridine / dichloromethane / 20 h / 25 °C / Inert atmosphere

With pyridine; dmap; palladium on activated charcoal; S-phenyl 4-methoxybenzenesulfinothioate; hydrogen; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/ja403323y