C₆₂H₆₇NO₂₄

Base Information

• Chemical Name: C₆₂H₆₇NO₂₄
• CAS No.: 1609475-89-9
• Molecular Formula: C₆₂H₆₇NO₂₄
• Molecular Weight: 1210.21
• Mol file: 1609475-89-9.mol

Synonyms:C₆₂H₆₇NO₂₄

Chemical Property of C₆₂H₆₇NO₂₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₂H₆₇NO₂₄

There total 2 articles about C₆₂H₆₇NO₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

N,N-dimethyl-2,5-bis[(trimethylsilyl)ethynyl]aniline (1609475-87-7) + C25H29IO12 (1609475-77-5) → C62H67NO24 (1609475-89-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide; at 70 ℃; for 7h;

DOI:10.1016/j.ejmech.2016.01.041

Reference yield: 61.0%

N,N-dimethyl-2,5-bis[(trimethylsilyl)ethynyl]aniline (1609475-87-7) + C25H29IO12 (1609475-77-5) → C62H67NO24 (1609475-89-9) + C54H58O24 (1609475-82-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; In tetrahydrofuran; N,N-dimethyl-formamide; for 7h; Inert atmosphere;

DOI:10.1021/jo500661u

Reference yield: 97.0%

C62H67NO24 (1609475-89-9) → C46H51NO16 (1609475-91-3)

Guidance literature:

With ammonium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 16h;

DOI:10.1016/j.ejmech.2016.01.041

upstream raw materials:

N,N-dimethyl-2,5-bis[(trimethylsilyl)ethynyl]aniline

C₂₅H₂₉IO₁₂

Downstream raw materials:

C₄₆H₅₁NO₁₆