(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

Base Information

Chemical Name:(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid
CAS No.:475296-59-4
Molecular Formula:C₁₆H₂₁NO₅S
Molecular Weight:339.412
Hs Code.:

Synonyms:(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

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Chemical Property of (S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

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Technology Process of (S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

There total 1 articles about (S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 148680-16-4
(S)-3-carbonylbenzyloxy-4-(2-ethylsulfanylcarbonyl-ethyl)-oxazolidin-5-one

: 475296-59-4
(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1021/jo026722l

Reference yield: 100.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 475296-59-4
(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

: 475296-60-7
(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid methyl ester

Guidance literature:: DOI:10.1021/ol026799w DOI:10.1021/jo026722l

Reference yield:

: 475296-59-4
(S)-2-(benzyloxycarbonyl-methyl-amino)-4-ethylsulfanylcarbonyl-butyric acid

: (S)-5-Amino-2-(benzyloxycarbonyl-methyl-amino)-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃SiH / Pd/C / acetone / 1 h

2: ammonium acetate; NaCNBH₃ / methanol / 0.5 h / 20 °C

With ammonium acetate; triethylsilane; sodium cyanoborohydride; palladium on activated charcoal; In methanol; acetone;
DOI:10.1021/jo026722l