N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide
CAS No.:1403502-78-2
Molecular Formula:C₁₈H₁₈N₂O₄S
Molecular Weight:358.418
Hs Code.:

Synonyms:N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

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Technology Process of N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

There total 2 articles about N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1403502-77-1
2-vinyl-1,2,3,4-tetrahydronaphthalen-1-amine

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1403502-78-2
N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201204484

Reference yield:

: (E)-2-(p-toluenesulfonyl)-2,3,6,7-tetrahydro-1H-benzo[c]azonine

: 1403502-78-2
N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; hexane / 1.25 h / -78 - -20 °C / Inert atmosphere

2: naphthalene; lithium / tetrahydrofuran / 0.5 h / -78 - -10 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; n-butyllithium; naphthalene; lithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane; 1: |[2,3]-Wittig Rearrangement;
DOI:10.1002/anie.201204484

Reference yield: 92.0%

: 1403502-78-2
N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide

: 1403502-79-3
C₁₇H₁₆N₂O₅S

Guidance literature:: N-(2-vinyl-1,2,3,4-tetrahydronaphthalen-1-yl)-2-nitrobenzenesulfonamide; With ozone; In methanol; dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

With triphenylphosphine; In methanol; dichloromethane; at -78 - 0 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1002/anie.201204484