Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate

Base Information

Chemical Name:Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate
CAS No.:89278-31-9
Molecular Formula:C₂₉H₃₅NO₇
Molecular Weight:509.599
Hs Code.:

Synonyms:Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate

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Chemical Property of Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate

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Technology Process of Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate

There total 5 articles about Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 89278-30-8,89361-29-5
(E/Z)-8-Benzyloxy-6(S),7(S)-O-isopropylidene-4-octenal

: N-Benzyloxycarbonyl-2-(dimethoxyphosphinyl)glycinmethylester

: 89278-31-9
Methyl 10-Benzyloxy-2-(S)-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E/Z),6(E/Z)-decadienoate

Guidance literature:: With potassium tert-butylate; In dichloromethane; at -70 ℃; for 0.5h;

Reference yield:

: 81028-12-8
(4S,5R)-4-benzyloxymethyl-2,2-dimethyl-1,3-dioxolane-5-carboxaldehyde

: 89278-31-9,108146-58-3,108146-60-7
Methyl 10-benzyloxy-2-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(E),6(E/Z)-decadienoate

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) potassium t-butoxide / 1.) CH₂Cl₂, -70 deg C, 10 min, 2.) -70 deg C --> 35 deg C, 0.5 h

With potassium tert-butylate;
DOI:10.1055/s-1986-31636

Reference yield:

: 81028-12-8
(4S,5R)-4-benzyloxymethyl-2,2-dimethyl-1,3-dioxolane-5-carboxaldehyde

: 89278-31-9,108146-58-3,108146-60-7
Methyl 10-benzyloxy-2-benzyloxycarbonylamino-8(S),9(S)-O-isopropylidene-2(Z),6(Z/E)-decadienoate

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) potassium t-butoxide / 1.) CH₂Cl₂, -70 deg C, 10 min, 2.) -70 deg C --> 35 deg C, 0.5 h

With potassium tert-butylate;
DOI:10.1055/s-1986-31636