para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside

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Chemical Name:para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside
CAS No.:1158840-64-2
Molecular Formula:C₄₇H₅₄O₁₅
Molecular Weight:858.937
Hs Code.:

para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside

Synonyms:para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside

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Chemical Property of para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside

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Technology Process of para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside

There total 1 articles about para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: p-methoxyphenyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

: 1158840-53-9
methyl (phenyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-1-thio-β-D-mannopyranosyluronate)

: 1158840-64-2
para-methoxyphenyl 2-O-benzyl-4,6-benzylidene-4-O-[methyl (ethyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-α-D-mannopyranosyluronate)]-β-D-galactopyranoside

Guidance literature:: methyl (phenyl 2-O-benzyl-3,4-O-[2',3'-dimethoxybutane-2',3'-diyl]-1-thio-β-D-mannopyranosyluronate); With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 - -45 ℃; for 0.25h; Molecular sieve;

p-methoxyphenyl 2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside; In dichloromethane; at -60 - 20 ℃; stereoselective reaction; Molecular sieve;
DOI:10.1016/j.tet.2009.02.067