(Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

Base Information

Chemical Name:(Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate
CAS No.:1341209-11-7
Molecular Formula:C₂₅H₃₀N₂O₆
Molecular Weight:454.523
Hs Code.:

Synonyms:(Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

There total 3 articles about (Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₄N₂O₄

: 501-53-1,94274-21-2
benzyl chloroformate

: 1341209-11-7
(Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jm200614t

Reference yield:

: 911845-36-8
(2Z)-4-(5-bromo-2-nitrophenoxy)but-2-enyl propionate

: 1341209-11-7
(Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium fluoride; potassium carbonate / N,N-dimethyl-formamide / 14 h / 120 °C / Molecular sieve

2: tin(II) chloride dihdyrate / ethanol / 18 h / Inert atmosphere; Reflux

3: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; potassium fluoride; tin(II) chloride dihdyrate; potassium carbonate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm200614t

Reference yield:

: 1341209-09-3
(Z)-4-(5-morpholino-2-nitrophenoxy)but-2-enyl propionate

: 1341209-11-7
(Z)-4-(2-(benzyloxycarbonylamino)-5-morpholinophenoxy)but-2-enyl propionate

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride dihdyrate / ethanol / 18 h / Inert atmosphere; Reflux

2: pyridine / dichloromethane / 2 h / 20 °C

With pyridine; tin(II) chloride dihdyrate; In ethanol; dichloromethane;
DOI:10.1021/jm200614t