chlorosuccinic acid monobenzyl ester

Base Information

Chemical Name:chlorosuccinic acid monobenzyl ester
CAS No.:104754-28-1
Molecular Formula:C₁₁H₁₁ClO₄
Molecular Weight:242.659
Hs Code.:

Synonyms:chlorosuccinic acid monobenzyl ester

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Chemical Property of chlorosuccinic acid monobenzyl ester

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Technology Process of chlorosuccinic acid monobenzyl ester

There total 1 articles about chlorosuccinic acid monobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104754-29-2
1-benzyl 2-chlorosuccimic dicyclohexylammonium

: 104754-28-1
chlorosuccinic acid monobenzyl ester

Guidance literature:: With DOWEX 50W-X₄ cation-exchange resin; In water; acetone; for 1.16667h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96774-2

Reference yield: 100.0%

: 104754-28-1
chlorosuccinic acid monobenzyl ester

: 104754-30-5
1-benzyl 2-chlorosuccinyl chloride

Guidance literature:: With thionyl chloride; at 65 ℃; for 1.5h;
DOI:10.1016/S0040-4020(01)96774-2

Reference yield:

: 104754-28-1
chlorosuccinic acid monobenzyl ester

: 140176-83-6
benzyl (+/-)-2-phenyl-3-oxo-5-isoxazolidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / 70 °C

2: diethyl ether / 0.25 h

3: 48 percent / aq. sodium bicarbonate / diethyl ether / Ambient temperature

With thionyl chloride; sodium hydrogencarbonate; In diethyl ether;
DOI:10.1021/jo00036a013