N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Base Information

Chemical Name:N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide
CAS No.:1400701-08-7
Molecular Formula:C₂₄H₂₁ClN₆O₃
Molecular Weight:476.922
Hs Code.:

Synonyms:N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

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Chemical Property of N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

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Technology Process of N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

There total 7 articles about N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1400700-92-6
C₁₆H₁₆N₆O₃

: 99-91-2
para-chloroacetophenone

: 1400701-08-7
N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Guidance literature:: With acetic acid; In ethanol; for 5h; Reflux;
DOI:10.1016/j.ejmech.2012.06.048

Reference yield:

: 1400700-86-8
C₁₈H₁₈N₄O₄

: 1400701-08-7
N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 5 h / 20 °C

2: acetic acid / ethanol / 5 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/j.ejmech.2012.06.048

Reference yield:

: 103-71-9
phenyl isocyanate

: 1400701-08-7
N'-[1-(4-chlorophenyl)ethylidene]-1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1: dichloromethane

2: sodium tetrahydroborate / ethanol

3: benzene / 3 h / 20 °C

4: 2 h / Reflux

5: hydrazine hydrate / ethanol / 5 h / 20 °C

6: acetic acid / ethanol / 5 h / Reflux

With sodium tetrahydroborate; hydrazine hydrate; acetic acid; In ethanol; dichloromethane; benzene;
DOI:10.1016/j.ejmech.2012.06.048