octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

Base Information

Chemical Name:octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside
CAS No.:130524-17-3
Molecular Formula:C₅₉H₇₂O₁₂
Molecular Weight:973.213
Hs Code.:

Synonyms:octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

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Chemical Property of octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

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Technology Process of octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

There total 10 articles about octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 65827-59-0
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride

: 130524-12-8
octyl 4,8-anhydro-2,3-di-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

: 130524-17-3
octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; for 2.5h; Ambient temperature;

Reference yield:

: 111-87-5
octanol

: 130524-17-3
octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: 78 percent / silver zeolite / CH₂Cl₂ / 2 h / Ambient temperature

2: 97 percent / sodium methoxide / methanol / Ambient temperature

3: 74 percent / 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 1.) from 0 deg C to -18 deg C, 15 h, 2.) RT, 60 min

4: 63 percent / sodium hydride / dimethylformamide / 3 h / -50 - 20 °C

5: pyridine / CH₂Cl₂ / 0.33 h / -10 °C

6: dimethylformamide / 2 h / Ambient temperature

7: 64 mg / sodium methoxide / methanol / Ambient temperature

8: 66 percent / tetramethylurea, silver trifluoromethanesulfonate / CH₂Cl₂ / 2.5 h / Ambient temperature

With pyridine; dmap; silver zeolite; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; tetramethylurea; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 130524-07-1
octyl 2,3-di-O-benzyl-7-deoxy-L-glycero-β-D-gluco-octopyranoside

: 130524-17-3
octyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-manno-pyranosyl)-4,8-anhydro-2,3-O-benzyl-7-deoxy-D-glycero-β-D-gluco-octopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 74 percent / 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 1.) from 0 deg C to -18 deg C, 15 h, 2.) RT, 60 min

2: 63 percent / sodium hydride / dimethylformamide / 3 h / -50 - 20 °C

3: pyridine / CH₂Cl₂ / 0.33 h / -10 °C

4: dimethylformamide / 2 h / Ambient temperature

5: 64 mg / sodium methoxide / methanol / Ambient temperature

6: 66 percent / tetramethylurea, silver trifluoromethanesulfonate / CH₂Cl₂ / 2.5 h / Ambient temperature

With pyridine; dmap; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; tetramethylurea; In methanol; dichloromethane; N,N-dimethyl-formamide;