Tc(CN-t-Bu)6}(PF₆)

Base Information

Chemical Name:Tc(CN-t-Bu)6}(PF₆)
CAS No.:86767-65-9
Molecular Formula:C₃₀H₅₄N₆Tc*F₆P
Molecular Weight:741.67
Hs Code.:

Synonyms:Tc(CN-t-Bu)6}(PF₆)

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Chemical Property of Tc(CN-t-Bu)6}(PF₆)

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Technology Process of Tc(CN-t-Bu)6}(PF₆)

There total 1 articles about Tc(CN-t-Bu)6}(PF₆) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: ammonium hexafluorophosphate

: 34035-97-7
ammonium pertechnetate

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 86767-65-9
Tc(CN-t-Bu)6}(PF₆)

Guidance literature:: With NaOH; Na₂S₂O₄; In ethanol; water; mixt. of educts (pH adjusted to 12 with NaOH) was heated to reflux, pH 12 aq. soln. of Na2S2O4 was added dropwise over 5 min; refluxing for 30 min, addnl. soln. of Na2S2O4 was added dropwise, refluxing for 30 min, concn., adding of H2O and NH4PF6; filtration, washing with H2O and ether, drying in vac., recrystn. from acetone/water; elem. anal.;