C₂₄H₂₂F₉N₃O

Base Information

Chemical Name:C₂₄H₂₂F₉N₃O
CAS No.:1313745-89-9
Molecular Formula:C₂₄H₂₂F₉N₃O
Molecular Weight:539.444
Hs Code.:

C<sub>24</sub>H<sub>22</sub>F<sub>9</sub>N<sub>3</sub>O

Synonyms:C₂₄H₂₂F₉N₃O

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Chemical Property of C₂₄H₂₂F₉N₃O

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Technology Process of C₂₄H₂₂F₉N₃O

There total 2 articles about C₂₄H₂₂F₉N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313750-03-6
(S)-cyclopropanecarboxylic acid [1-(4-bromo-phenyl)-ethyl]-amide

: 1313750-01-4
2,6-bis(trifluoromethyl)-4-[3-(trifluoromethyl)pyrrolidin-3-yl]pyridine

: 1313745-89-9
C₂₄H₂₂F₉N₃O

Guidance literature:: With sodium t-butanolate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 120 ℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Sealed vessel;

Reference yield:

: 1254832-32-0
2,6-bis(trifluoromethyl)-4-(3,3,3-trifluoroprop-1-en-2-yl)pyridine

: 1313745-89-9
C₂₄H₂₂F₉N₃O

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 20 °C / Cooling with ice

2.1: carbonochloridic acid 1-chloro-ethyl ester / 1,1-dichloroethane / 3 h / Reflux

2.2: 2 h / 60 °C

3.1: sodium t-butanolate / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / toluene / 0.17 h / 120 °C / Microwave irradiation; Inert atmosphere; Sealed vessel

With carbonochloridic acid 1-chloro-ethyl ester; trifluoroacetic acid; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,1-dichloroethane; dichloromethane; toluene;