(-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate)

Base Information

• Chemical Name: (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate)
• CAS No.: 1262331-27-0
• Molecular Formula: C₆₅H₆₉O₁₇P₃
• Molecular Weight: 1215.17

Synonyms:(-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate)

Chemical Property of (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate)

Chemical Property:

Purity/Quality:

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Technology Process of (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate)

There total 6 articles about (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C65H69O16P3 → (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate) (1262331-27-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; at -78 - 20 ℃; for 1.25h; Inert atmosphere;

DOI:10.1039/c0cc03003a

Reference yield:

(-)-D-3-O-benzyl-2,6-O-bisbenzyloxymethyl-5-O-(4-methoxybenzyl)-4-O-triisopropylsilyl-myo-inositol (1169763-42-1) → (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate) (1262331-27-0)

Guidance literature:

Multi-step reaction with 6 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.25 h / Inert atmosphere

2.2: 18 h / 20 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; acetonitrile / 1.75 h / -78 - 20 °C / Inert atmosphere

4.1: ammonium cerium (IV) nitrate; water / acetonitrile / 0.67 h

5.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.17 h / Inert atmosphere

5.2: 18 h / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; acetonitrile / 1.25 h / -78 - 20 °C / Inert atmosphere

With 1H-tetrazole; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; water; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetonitrile;

DOI:10.1039/c0cc03003a

Reference yield:

(-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-5-O-(4-methoxybenzyl)-D-myo-inositol (1169763-46-5) → (-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate) 5-(benzyl methyl phosphate) (1262331-27-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.25 h / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; acetonitrile / 1.75 h / -78 - 20 °C / Inert atmosphere

3.1: ammonium cerium (IV) nitrate; water / acetonitrile / 0.67 h

4.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.17 h / Inert atmosphere

4.2: 18 h / Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; acetonitrile / 1.25 h / -78 - 20 °C / Inert atmosphere

With 1H-tetrazole; ammonium cerium (IV) nitrate; water; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;

DOI:10.1039/c0cc03003a

upstream raw materials:

(-)-D-3-O-benzyl-2,6-O-bisbenzyloxymethyl-5-O-(4-methoxybenzyl)-4-O-triisopropylsilyl-myo-inositol

(-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-5-O-(4-methoxybenzyl)-D-myo-inositol

(-)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-5-O-(4-methoxybenzyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate)

(+)-3-O-benzyl-2,6-bis-O-(benzyloxymethyl)-D-myo-inositol 1,4-bis(dibenzyl phosphate)

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