7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine

Base Information

Chemical Name:7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine
CAS No.:57616-51-0
Molecular Formula:C₂₁H₂₁Cl₂N₃S
Molecular Weight:418.39
Hs Code.:

7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3<i>H</i>-benzo[<i>e</i>][1,4]diazepine

Synonyms:7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine

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Chemical Property of 7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine

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Technology Process of 7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine

There total 3 articles about 7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7250-67-1
1-(2-chloroethyl)pyrrolidine hydrochloride

: 2894-71-5,49853-64-7
7-chloro-1,3-dihydro-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione

: 57616-52-1
2-[2-(1-pyrrolidinyl)ethylthio]-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine fumarate

: 57616-51-0
7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine

Guidance literature:: With sodium hydroxide; In methanol;

Reference yield:

: 7250-67-1
1-(2-chloroethyl)pyrrolidine hydrochloride

: 2894-71-5,49853-64-7
7-chloro-1,3-dihydro-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione

: 57616-51-0
7-chloro-5-(2-chloro-phenyl)-2-(2-pyrrolidin-1-yl-ethylsulfanyl)-3H-benzo[e][1,4]diazepine

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; water; for 1.5h; Yield given; Ambient temperature;
DOI:10.1248/cpb.30.1141