Technology Process of C29H26N2O5
There total 4 articles about C29H26N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1039/c2cc36011j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; acetic acid / dichloromethane / 3 h / 20 °C
2: tetrabutylammomium bromide; potassium carbonate / dichloromethane; water / 1 h / 0 °C
3: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
With
(2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; tetrabutylammomium bromide; potassium carbonate; acetic acid; pyridinium chlorochromate;
In
dichloromethane; water;
1: |Michael Addition;
DOI:10.1039/c2cc36011j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; acetic acid / dichloromethane / 3 h / 20 °C
2: tetrabutylammomium bromide; potassium carbonate / dichloromethane; water / 1 h / 0 °C
3: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
With
(2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; tetrabutylammomium bromide; potassium carbonate; acetic acid; pyridinium chlorochromate;
In
dichloromethane; water;
1: |Michael Addition;
DOI:10.1039/c2cc36011j
