<2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

Base Information

Chemical Name:<2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide
CAS No.:59043-74-2
Molecular Formula:BrH*C₁₀H₁₄FNO₂
Molecular Weight:280.137
Hs Code.:

Synonyms:<2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

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Chemical Property of <2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

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Technology Process of <2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

There total 6 articles about <2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 72912-24-4
2-fluoro-3,4-dimethoxyphenethyl amine

: 59043-74-2
<2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

Guidance literature:: With hydrogen bromide; In ethanol;
DOI:10.1021/jo00314a054

Reference yield:

: 456-49-5
1-fluoro-3-methoxybenzene

: 59043-74-2
<2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

Guidance literature:: Multi-step reaction with 6 steps

2: 68 percent / K₂CO₃ / acetone / 4 h reflux, standing overnight, 1 h reflux

3: 95 percent / HCl / acetic acid / 4.5 h / 20 - 25 °C

4: 92 percent / dimethylsulfoxide / 0.75 h

5: 76 percent / BH₃ / tetrahydrofuran / 1.5 h / Heating

6: 64 percent / HBr / ethanol

With hydrogenchloride; borane; hydrogen bromide; potassium carbonate; In tetrahydrofuran; ethanol; acetic acid; dimethyl sulfoxide; acetone;
DOI:10.1021/jo00314a054

Reference yield:

: 394-64-9
1-fluoro-2,3-dimethoxybenzene

: 59043-74-2
<2-(2-fluoro-3,4-dimethoxyphenyl)ethyl>amine hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / HCl / acetic acid / 4.5 h / 20 - 25 °C

2: 92 percent / dimethylsulfoxide / 0.75 h

3: 76 percent / BH₃ / tetrahydrofuran / 1.5 h / Heating

4: 64 percent / HBr / ethanol

With hydrogenchloride; borane; hydrogen bromide; In tetrahydrofuran; ethanol; acetic acid; dimethyl sulfoxide;
DOI:10.1021/jo00314a054