(S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

Base Information

Chemical Name:(S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid
CAS No.:130932-95-5
Molecular Formula:C₃₂H₄₅N₅O₁₁
Molecular Weight:675.736
Hs Code.:

(S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

Synonyms:(S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

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Chemical Property of (S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

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Technology Process of (S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

There total 1 articles about (S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 24695-48-5
1-(5'-amino-5'-deoxy-α-D-allofuranuronosyl)uracil

: 100566-81-2
N-α-(benzyloxycarbonyl)-N-ε-octanoyllysine p-nitrophenyl ester

: 130932-95-5
(S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

Guidance literature:: With diisopropylamine; In dimethyl sulfoxide; for 20h; Ambient temperature;
DOI:10.1021/jm00105a026

Reference yield:

: 130932-95-5
(S)-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

: (S)-[(S)-2-((S)-2-Benzyloxycarbonylamino-6-octanoylamino-hexanoylamino)-6-octanoylamino-hexanoylamino]-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 78 mg / 90percent formic acid / Pd / methanol

2: N-methylmorpholine / dimethylformamide / 15 h / Ambient temperature

With 4-methyl-morpholine; formic acid; palladium; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00105a026