[4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

Base Information

Chemical Name:[4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]
CAS No.:426213-22-1
Molecular Formula:C₅₁H₃₉Au₂BrO₂P₂
Molecular Weight:1219.65
Hs Code.:

Synonyms:[4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

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Technology Process of [4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

There total 5 articles about [4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: BrC₆H₄CH(C₆H₄OCH₂C₂Au)2

: 983-81-3
trans-1,2-bis(diphenylphosphino)ethylene

: 426213-22-1
[4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

Guidance literature:: In dichloromethane; the mixt. in CH2Cl2 was stirred at room temp. in a darkened reaction flask for 2 h, activated charcoal was added and the mixt. was stirred for 0.5 h; filtered, the solvent was removed under reduced pressure, recrystd. fromCH2Cl2-pentane; elem. anal.;
DOI:10.1021/ja012006+

Reference yield:

: 426213-18-5
BrC₆H₄CH(C₆H₄OCH₂C₂H)2

: 426213-22-1
[4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

Guidance literature:: Multi-step reaction with 2 steps

1: NaOOCCH₃ / tetrahydrofuran; methanol

2: dichloromethane

With NaOOCCH₃; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja012006+

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 426213-22-1
[4-BrC6H4CH(4-C6H4OCH2CCAu)2(μ-trans-bis(diphenylphosphino)ethylene)]

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; acetic acid / 72 h / 0 °C

2: potassium hydroxide / acetone / 16 h / Heating

3: NaOOCCH₃ / tetrahydrofuran; methanol

4: dichloromethane

With potassium hydroxide; sulfuric acid; acetic acid; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1021/ja012006+