2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

Base Information

Chemical Name:2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide
CAS No.:181820-96-2
Molecular Formula:C₂₀H₁₉N₃O₃S
Molecular Weight:381.455
Hs Code.:

Synonyms:2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

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Chemical Property of 2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

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Technology Process of 2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

There total 5 articles about 2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 181823-64-3
2-[1-(2-Methoxy-phenyl)-ethylsulfanyl]-N-pyridin-4-yl-nicotinamide

: 181820-96-2
2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.05h;

Reference yield:

: 504-24-5
4-aminopyridine

: 181820-96-2
2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Et₃N=C=N(CH₂)3NMe₂*HCl / CH₂Cl₂ / 3 h / Ambient temperature

2: 17 percent / m-CPBA / CH₂Cl₂ / 0.05 h / 0 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

: 38521-46-9
3-carboxy-2-mercaptopyridine

: 181820-96-2
2-[(2-methoxy-α-methylbenzyl)sulfinyl]-N-(4-pyridinyl)-3-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / cc. HCl / acetone / 3 h / Ambient temperature

2: 76 percent / Et₃N=C=N(CH₂)3NMe₂*HCl / CH₂Cl₂ / 3 h / Ambient temperature

3: 17 percent / m-CPBA / CH₂Cl₂ / 0.05 h / 0 °C

With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetone;