methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

Base Information

Chemical Name:methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate
CAS No.:1040185-03-2
Molecular Formula:C₂₀H₂₈N₂O₆
Molecular Weight:392.452
Hs Code.:

Synonyms:methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

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Chemical Property of methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

Chemical Property:

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Technology Process of methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

There total 1 articles about methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1040185-21-4
(5-formylpyridin-2-yl)dicarbamic acid tert-butyl ester

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 1040185-03-2
methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

Guidance literature:: glycine ethyl ester hydrochloride; With magnesium sulfate; triethylamine; In dichloromethane; at 20 ℃;

(5-formylpyridin-2-yl)dicarbamic acid tert-butyl ester; In dichloromethane; at 20 ℃;
DOI:10.1021/ja804021m

Reference yield: 75.0%

: 1040185-03-2
methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

: 1865-13-0,63068-63-3,91077-67-7
(Z)-β-phenylsulphonylacrylic acid methyl ester

: C₃₀H₃₈N₂O₁₀S

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; triethylamine; triphenylphosphine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201000742

Reference yield:

: 1040185-03-2
methyl (E)-N-[(p-(di-(tert-butoxycarbonyl)amino)phenyl)methylene]glycinate

: 1865-13-0,63068-63-3,91077-67-7
(Z)-β-phenylsulphonylacrylic acid methyl ester

: 1130894-33-5
(2R,3R,4S,5R)-dimethyl 5-[(p-di(tert-butoxycarbonyl)amino)phenyl]-4-(phenylsulfonyl)pyrrolidine-2,3-dicarboxylate

: (2S,3S,4R,5S)-dimethyl 5-[(p-di(tert-butoxycarbonyl)amino)phenyl]-4-(phenylsulfonyl)pyrrolidine-2,3-dicarboxylate

Guidance literature:: With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; tetrakis(actonitrile)copper(I) hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃; optical yield given as %ee; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200805063