C₁₂H₁₃ClO₂

Base Information

• Chemical Name: C₁₂H₁₃ClO₂
• CAS No.: 1364301-61-0
• Molecular Formula: C₁₂H₁₃ClO₂
• Molecular Weight: 224.687
• Mol file: 1364301-61-0.mol

Synonyms:C₁₂H₁₃ClO₂

Chemical Property of C₁₂H₁₃ClO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₂H₁₃ClO₂

There total 1 articles about C₁₂H₁₃ClO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-iodo-2-chloropropene (39557-31-8) + methyl 2-iodo-5-methylbenzoate (103440-52-4) → C12H13ClO2 (1364301-61-0)

Guidance literature:

methyl 2-iodo-5-methylbenzoate; With isopropylmagnesium bromide; In tetrahydrofuran; at -40 ℃; for 0.5h; Inert atmosphere;

With copper(l) cyanide; lithium chloride; In tetrahydrofuran; at -40 ℃; for 0.0833333h; Inert atmosphere;

3-iodo-2-chloropropene; In tetrahydrofuran; at -40 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.01.011

Reference yield:

C12H13ClO2 (1364301-61-0) → C11H11ClO2 (1364301-72-3)

Guidance literature:

C₁₂H₁₃ClO₂; With sodium hydroxide; In methanol; water; at 20 ℃; for 20h;

With hydrogenchloride; In water; pH=2;

DOI:10.1016/j.tetlet.2012.01.011

upstream raw materials:

3-iodo-2-chloropropene

methyl 2-iodo-5-methylbenzoate

Downstream raw materials:

C₁₁H₁₁ClO₂

Refernces