[((C₆H₅)2NC₆H₄CCPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole]

Base Information

• Chemical Name: [((C₆H₅)2NC₆H₄CCPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole]
• CAS No.: 1139887-56-1
• Molecular Formula: C₈₂H₉₆N₄OP₄Pt₂
• Molecular Weight: 1667.75
• Mol file: 1139887-56-1.mol

Synonyms:[((C₆H₅)2NC₆H₄CCPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole]

Chemical Property of [((C₆H₅)2NC₆H₄CCPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [((C₆H₅)2NC₆H₄CCPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole]

There total 1 articles about [((C₆H₅)2NC₆H₄CCPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

[(ClPt(PEt3)2CC)2-2,5-diphenyl-1,3,4-oxadiazole] (1139887-54-9) + 4-diphenylaminophenylacetylene (205877-26-5) → [((C6H5)2NC6H4CCPt(PEt3)2CC)2-2,5-diphenyl-1,3,4-oxadiazole] (1139887-56-1)

Guidance literature:

With triethylamine; copper(l) iodide; In tetrahydrofuran; to soln. Pt complex and alkyne in THF-Et3N CuI was added and stirred overnight at room temp. under N2 atm.; solvent was removed in vacuo, residue was dissolved in CH2Cl2, washed with brine and water, dried over Na2SO4, filtered and evapd. in vacuo, residue was chromd. on basic alumina (CH2Cl2) and recrystd. from CH2Cl2-n-hexane; elem. anal.;

DOI:10.1021/ic8017979

upstream raw materials:

[(ClPt(PEt₃)2CC)2-2,5-diphenyl-1,3,4-oxadiazole]

4-diphenylaminophenylacetylene