2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

Base Information

Chemical Name:2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether
CAS No.:854300-80-4
Molecular Formula:C₄₂H₈₀O₁₃P₂
Molecular Weight:855.037
Hs Code.:

Synonyms:2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

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Technology Process of 2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

There total 4 articles about 2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 854300-84-8
Phosphorous acid 2-benzyloxy-3-[((R)-2,3-bis-hexyloxy-propoxy)-methoxy-phosphanyloxy]-propyl ester (R)-2,3-bis-hexyloxy-propyl ester methyl ester

: 854300-80-4
2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; at -40 ℃;

Reference yield:

: 124186-29-4
(2R)-3-O-benzyl-1,2-di-O-hexyl-sn-glycerol

: 854300-80-4
2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / H₂ / Pd/C / ethyl acetate / 4 h

2: N,N-diisopropylethylamine / CH₂Cl₂ / 2 h / 20 °C

3: 1H-tetrazole / CH₂Cl₂ / 6 h / 20 °C

4: m-chloroperbenzoic acid / 1 h / -40 °C

With 1H-tetrazole; hydrogen; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2005.03.046

Reference yield:

: 854300-83-7
1,2-di-O-hexyl-sn-glycero-N,N-diisopropyl methylphosphoramidite

: 854300-80-4
2-O-benzyl-1,3-bis-(1,2-di-O-hexyl-sn-glycero-3-phosphoryl)glycerol dimethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂ / 6 h / 20 °C

2: m-chloroperbenzoic acid / 1 h / -40 °C

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2005.03.046