C₆₁H₆₂O₁₀SSi

Base Information

Chemical Name:C₆₁H₆₂O₁₀SSi
CAS No.:1360560-51-5
Molecular Formula:C₆₁H₆₂O₁₀SSi
Molecular Weight:1015.31
Hs Code.:

C<sub>61</sub>H<sub>62</sub>O<sub>10</sub>SSi

Synonyms:C₆₁H₆₂O₁₀SSi

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Chemical Property of C₆₁H₆₂O₁₀SSi

Chemical Property:

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Technology Process of C₆₁H₆₂O₁₀SSi

There total 6 articles about C₆₁H₆₂O₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917590-91-1
p-tolyl 2,3-di-O-benzyl-5-O-(tert-butyldiphenylsilyl)-1-thio-α-D-arabinofuranoside

: 685111-68-6
p-toluyl 2,3-di-O-benzoyl-1-thio-α-D-arabinofuranoside

: 1360560-51-5
C₆₁H₆₂O₁₀SSi

: C₆₁H₆₂O₁₀SSi

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In EtCN; dichloromethane; acetonitrile; at -70 ℃; for 0.5h; optical yield given as %de; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201100732

Reference yield:

: 204918-49-0
p-methylphenyl 1-thio-α-D-arabinofuranoside

: 1360560-51-5
C₆₁H₆₂O₁₀SSi

: C₆₁H₆₂O₁₀SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2.17 h / 0 - 20 °C / Inert atmosphere

2: pyridine / 0 - 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride; trifluoroacetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / EtCN; dichloromethane; acetonitrile / 0.5 h / -70 °C / Inert atmosphere; Molecular sieve

With pyridine; 1H-imidazole; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; trifluoroacetic acid; In tetrahydrofuran; EtCN; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201100732

Reference yield:

: 204918-55-8
p-cresyl 5-O-tert-butyldiphenylsilyl-1-thio-α-D-arabinofuranoside

: 1360560-51-5
C₆₁H₆₂O₁₀SSi

: C₆₁H₆₂O₁₀SSi

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride; trifluoroacetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / EtCN; dichloromethane; acetonitrile / 0.5 h / -70 °C / Inert atmosphere; Molecular sieve

With pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; trifluoroacetic acid; In tetrahydrofuran; EtCN; dichloromethane; acetonitrile;
DOI:10.1002/chem.201100732