Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

Base Information

Chemical Name:Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester
CAS No.:206053-74-9
Molecular Formula:C₄₇H₅₅NO₁₁
Molecular Weight:809.954
Hs Code.:

Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

Synonyms:Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

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Chemical Property of Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

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Technology Process of Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

There total 2 articles about Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 206053-74-9
Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃ / dimethylformamide / 1.) 0 deg C, 12 h, 2.) 20 deg C, 24 h

2: 1.) DMAP, NEt₃, 2.) DIPEA / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 deg C, 12 h

With dmap; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(98)00105-7

Reference yield:

: 181629-30-1
3-(tri-O-benzyl-α-L-fucopyranosyl)-1-propyl bromide

: 206053-74-9
Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃ / dimethylformamide / 1.) 0 deg C, 12 h, 2.) 20 deg C, 24 h

2: 1.) DMAP, NEt₃, 2.) DIPEA / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 deg C, 12 h

With dmap; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(98)00105-7

Reference yield: 65.0%

: 206053-74-9
Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

: Piperidine-1,4-dicarboxylic acid 4-ethyl ester 1-{3-methoxycarbonyl-5-[3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yl)-propoxy]-phenyl} ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; acetic acid; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(98)00105-7