C₁₄H₁₃FN₆

Base Information

Chemical Name:C₁₄H₁₃FN₆
CAS No.:1344669-92-6
Molecular Formula:C₁₄H₁₃FN₆
Molecular Weight:284.296
Hs Code.:

C<sub>14</sub>H<sub>13</sub>FN<sub>6</sub>

Synonyms:C₁₄H₁₃FN₆

Suppliers and Price of C₁₄H₁₃FN₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₃FN₆

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₃FN₆

There total 10 articles about C₁₄H₁₃FN₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27427-92-5
pyrimidine-2-carbaldehyde

: 1344669-92-6
C₁₄H₁₃FN₆

Guidance literature:: Multi-step reaction with 10 steps

1: isopropyl alcohol / 50 °C

2: caesium carbonate / tetrahydrofuran; isopropyl alcohol

3: hydrogenchloride / water

4: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 75 °C

5: ammonium acetate; ammonium hydroxide; zinc / ethanol; water / 80 °C

6: N-ethyl-N,N-diisopropylamine / dichloromethane

7: trichlorophosphate / 100 °C

8: ammonia / methanol

9: trifluoroacetic anhydride / tetrahydrofuran; pyridine

10: hydrazine hydrate / methanol

With hydrogenchloride; hydroxylamine hydrochloride; ammonium acetate; ammonia; caesium carbonate; ammonium hydroxide; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; sodium hydroxide; zinc; trichlorophosphate; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; isopropyl alcohol; 2: Horner-Emmons condensation;
DOI:10.1016/j.bmcl.2011.08.071

Reference yield:

: C₁₈H₁₄FN₃

: 1344669-92-6
C₁₄H₁₃FN₆

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / water

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 75 °C

3: ammonium acetate; ammonium hydroxide; zinc / ethanol; water / 80 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane

5: trichlorophosphate / 100 °C

6: ammonia / methanol

7: trifluoroacetic anhydride / tetrahydrofuran; pyridine

8: hydrazine hydrate / methanol

With hydrogenchloride; hydroxylamine hydrochloride; ammonium acetate; ammonia; ammonium hydroxide; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; sodium hydroxide; zinc; trichlorophosphate; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.08.071

Reference yield:

: 1426309-21-8
8-(2-fluorobenzyl)imidazo[1,5-a]pyrimidine-6-carboxamide

: 1344669-92-6
C₁₄H₁₃FN₆

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic anhydride / tetrahydrofuran; pyridine

2: hydrazine hydrate / methanol

With hydrazine hydrate; trifluoroacetic anhydride; In tetrahydrofuran; pyridine; methanol;
DOI:10.1016/j.bmcl.2011.08.071