3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

Base Information

Chemical Name:3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone
CAS No.:143302-99-2
Molecular Formula:C₂₅H₂₆O₇S₂
Molecular Weight:502.609
Hs Code.:

Synonyms:3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

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Chemical Property of 3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

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Technology Process of 3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

There total 3 articles about 3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 142836-54-2
2-(6-hydroxy-2,3,4-trimethoxybenzyl)-3-(3',4'-methylenedioxybenzoylpropane-1,3-dithiane)-γ-butyrolactone

: 143302-99-2
3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 56579-86-3
2-(3,4-methylenedioxyphenyl)-1,3-dithiane

: 143302-99-2
3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi

2: 83 percent / TFA / CH₂Cl₂ / 2 h / 0 °C

With n-butyllithium; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 2103-57-3
2,3,4-trimethoxybenzaldehyde

: 143302-99-2
3-hydroxymethyl-4-propane-1,3-dithiane-6,7-methylenedioxy-1-(2',3',4'-trimethoxyphenyl)-1,2,3,4-tetrahydro-2-naphthoic acid-γ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi

2: 83 percent / TFA / CH₂Cl₂ / 2 h / 0 °C

With n-butyllithium; trifluoroacetic acid; In dichloromethane;