BETA-D-GLCNAC-[1->3]-BETA-D-GAL-1->OME

Base Information

• Chemical Name: BETA-D-GLCNAC-[1->3]-BETA-D-GAL-1->OME
• CAS No.: 93253-17-9
• Molecular Formula: C₁₅H₂₇NO₁₁
• Molecular Weight: 397.379
• Hs Code.: 29389090
• Mol file: 93253-17-9.mol

Synonyms:BETA-D-GLCNAC-[1->3]-BETA-D-GAL-1->OME;METHYL 3-O-(2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSYL)-BETA-D-GALACTOPYRANOSIDE;methyl 3-O-(2-acetamido-2-deoxy-B-D-*glucopyranos;METHYL 3-O-(2-ACETAMIDO-2-DEOXY-B-D-*GLU COPYRANOSYL;methyl 3-o-(n-acetyl-尾-d-glucosaminyl)-尾-d-galactopyranoside;尾-d-glcnac-(1鈫?)-尾-d-gal-1鈫抩me;Methyl3-O-(2-acetamido-2-deoxy-b-glucopyranosyl)-b-D-galactopyranoside

Chemical Property of BETA-D-GLCNAC-[1->3]-BETA-D-GAL-1->OME

Chemical Property:

• Vapor Pressure: 1.52E-27mmHg at 25°C
• Refractive Index: 1.59
• Boiling Point: 772.3°C at 760 mmHg
• Flash Point: 420.9°C
• PSA: 187.40000
• Density: 1.54g/cm³
• LogP: -4.20840
• Storage Temp.: −20°C

Purity/Quality:

98% ^*data from raw suppliers

Methyl3-O-(N-Acetyl-β-D-glucosaminyl)-β-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Methyl 3-O-(N-Acetyl-β-D-glucosaminyl)-β-D-galactopyranoside is used in the preparation of disaccharide mucin fragment β-6-GlcNAc-transferase. Used in the preparation of disaccharide mucin fragment and for the inhibition studies of rat lung lectin. It is a substrate for β-6-GlcNAc-transferase.

Technology Process of BETA-D-GLCNAC-[1->3]-BETA-D-GAL-1->OME

There total 16 articles about BETA-D-GLCNAC-[1->3]-BETA-D-GAL-1->OME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

methyl 3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-β-D-galactopyranoside (98151-21-4) → GlcNAcβ1→3-Galβ-methyl (80599-53-7,88676-07-7,109303-71-1,128396-53-2,130234-66-1,130234-67-2,138492-84-9,138492-85-0,143657-27-6,146365-40-4,93253-17-9)

Guidance literature:

With sodium methylate; In methanol; Ambient temperature;

DOI:10.1016/0008-6215(85)85219-8

Reference yield: 90.0%

methyl 3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2,4,6-tri-O-acetyl-β-D-galactopyranoside (93253-18-0) → GlcNAcβ1→3-Galβ-methyl (80599-53-7,88676-07-7,109303-71-1,128396-53-2,130234-66-1,130234-67-2,138492-84-9,138492-85-0,143657-27-6,146365-40-4,93253-17-9)

Guidance literature:

With sodium methylate; In methanol; for 20h; Ambient temperature;

DOI:10.1016/S0008-6215(97)10093-3

Reference yield: 75.0%

methyl O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1-3)-2,4,6-tri-O-benzyl-β-galactopyranosyl (93253-16-8) → GlcNAcβ1→3-Galβ-methyl (80599-53-7,88676-07-7,109303-71-1,128396-53-2,130234-66-1,130234-67-2,138492-84-9,138492-85-0,143657-27-6,146365-40-4,93253-17-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; for 20h; under 2587.7 Torr; Ambient temperature;

DOI:10.1016/0008-6215(84)85070-3

upstream raw materials:

methyl O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1-3)-2,4,6-tri-O-benzyl-β-galactopyranosyl

methyl 3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-β-D-galactopyranoside

methyl beta-D-galactopyranoside

4-nitrophenyl N-acetyl-β-D-glucosaminide

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