(S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate

Base Information

• Chemical Name: (S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate
• CAS No.: 1149580-15-3
• Molecular Formula: C₃₀H₃₂F₂N₄O₇
• Molecular Weight: 598.603

Synonyms:(S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate

Chemical Property of (S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate

Chemical Property:

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Technology Process of (S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate

There total 1 articles about (S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(S)-benzyl 4-(3-(2,3-bis(benzyloxycarbonyl)guanidino)-2,2-difluoropropyl)-2,2-dimethyloxazolidine-3-carboxylate (1149580-14-2) → (S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate (1149580-15-3)

Guidance literature:

With boron trifluoride diethyl etherate; ethane-1,2-dithiol; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.bmcl.2009.01.076

Reference yield: 96.0%

(S)-benzyl 5-(bis(benzyloxycarbonyl)guanidino)-4,4-difluoro-1-hydroxypentan-2-ylcarbamate (1149580-15-3) → N(G),N'(G)-bis(benzyloxycarbonyl)-4,4-difluoro-Nα-benzyloxycarbonyl-L-arginine (1149580-16-4)

Guidance literature:

With chromium(VI) oxide; periodic acid; In water; acetonitrile; Cooling with ice;

DOI:10.1016/j.bmcl.2009.01.076

upstream raw materials:

(S)-benzyl 4-(3-(2,3-bis(benzyloxycarbonyl)guanidino)-2,2-difluoropropyl)-2,2-dimethyloxazolidine-3-carboxylate

Downstream raw materials:

N(G),N'(G)-bis(benzyloxycarbonyl)-4,4-difluoro-Nα-benzyloxycarbonyl-L-arginine

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