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Technology Process of Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6

Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6

Base Information
  • Chemical Name:Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6
  • CAS No.:1354725-79-3
  • Molecular Formula:C37H46N5PdSe*F6P
  • Molecular Weight:891.15
  • Hs Code.:
Pd((C<sub>2</sub>H<sub>5</sub>)2NC(Se)NC(C<sub>6</sub>H<sub>5</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)((CH<sub>3</sub>)3CC<sub>5</sub>H<sub>3</sub>N)2<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[Pd((C<sub>2</sub>H<sub>5</sub>)2NC(Se)NC(C<sub>6</sub>H<sub>5</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)((CH<sub>3</sub>)3CC<sub>5</sub>H<sub>3</sub>N)2]PF<sub>6</sub>

Synonyms:Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6

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Chemical Property of Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6
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Technology Process of Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6

There total 1 articles about Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

ammonium hexafluorophosphate

ammonium hexafluorophosphate

dichloro(4,4'-di-tert-butyl-2,2'-bipyridine)palladium(II)
162379-72-8

dichloro(4,4'-di-tert-butyl-2,2'-bipyridine)palladium(II)

(C<sub>2</sub>H<sub>5</sub>)2NC(Se)NC(C<sub>6</sub>H<sub>5</sub>)NHC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>
1355465-82-5

(C2H5)2NC(Se)NC(C6H5)NHC6H4CH3

Pd((C<sub>2</sub>H<sub>5</sub>)2NC(Se)NC(C<sub>6</sub>H<sub>5</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)((CH<sub>3</sub>)3CC<sub>5</sub>H<sub>3</sub>N)2<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[Pd((C<sub>2</sub>H<sub>5</sub>)2NC(Se)NC(C<sub>6</sub>H<sub>5</sub>)NC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)((CH<sub>3</sub>)3CC<sub>5</sub>H<sub>3</sub>N)2]PF<sub>6</sub>
1354725-79-3

Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2(1+)*PF6(1-)=[Pd((C2H5)2NC(Se)NC(C6H5)NC6H4CH3)((CH3)3CC5H3N)2]PF6

Guidance literature:
With triethyl amine; In methanol; benzamidine compd. and Et3N added to suspn. of Pd complex in MeOH contg.NH4PF6, mixt. heated at reflux for 15 min; soln. filtered, filtrate evapd. under vac., residue washed with H2O and Et2O, filtered, dried; elem. anal.;
DOI:10.1016/j.poly.2011.11.008
upstream raw materials:

dichloro(4,4'-di-tert-butyl-2,2'-bipyridine)palladium(II)

(C2H5)2NC(Se)NC(C6H5)NHC6H4CH3

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