(+/-)-N-benzoyl-α-vunylalanine methyl ester

Base Information

Chemical Name:(+/-)-N-benzoyl-α-vunylalanine methyl ester
CAS No.:74761-84-5
Molecular Formula:C₁₃H₁₅NO₃
Molecular Weight:233.267
Hs Code.:

Synonyms:(+/-)-N-benzoyl-α-vunylalanine methyl ester

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Chemical Property of (+/-)-N-benzoyl-α-vunylalanine methyl ester

Chemical Property:

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Technology Process of (+/-)-N-benzoyl-α-vunylalanine methyl ester

There total 9 articles about (+/-)-N-benzoyl-α-vunylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74806-83-0
(E)-4-Benzenesulfonyl-2-benzoylamino-2-methyl-but-3-enoic acid methyl ester

: 74761-84-5
(+/-)-N-benzoyl-α-vunylalanine methyl ester

Guidance literature:: With aluminium amalgam; In tetrahydrofuran; water; at 70 ℃; for 4h;
DOI:10.1055/s-1980-29063

Reference yield:

: 51127-13-0,71963-72-9,87480-74-8,13302-43-7
2-phenyl-4-methyl-4H-oxazolin-5-one

: 74761-84-5
(+/-)-N-benzoyl-α-vunylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Triethylamin / CH₂Cl₂ / 0.75 h / -20 °C

2: Triethylamin / 22 °C

3: Al-Hg / tetrahydrofuran; H₂O / 4 h / 70 °C

With aluminium amalgam; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1055/s-1980-29063

Reference yield:

: 74761-79-8
4-((E)-2-Benzenesulfonyl-vinyl)-4-methyl-2-phenyl-4H-oxazol-5-one

: 74761-84-5
(+/-)-N-benzoyl-α-vunylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Triethylamin / 22 °C

2: Al-Hg / tetrahydrofuran; H₂O / 4 h / 70 °C

With aluminium amalgam; triethylamine; In tetrahydrofuran; water;
DOI:10.1055/s-1980-29063