N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

Base Information

Chemical Name:N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine
CAS No.:108827-21-0
Molecular Formula:C₄₇H₆₂N₆O₁₀
Molecular Weight:871.043
Hs Code.:

Synonyms:N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

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Chemical Property of N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

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Technology Process of N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

There total 3 articles about N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108827-20-9
Z-D-Trp-Lys(Boc)-Thr(t-Bu)-Phe-OMe

: 108827-21-0
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 108827-48-1
N^ε-t-butoxycarbonyl-lysyl-O-t-butylthreonyl-phenylalanine methyl ester

: 108827-21-0
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1.) HOBt, DCC; 2.) DIEA / dimethylformamide / 16 h / 4 °C

2: 99 percent / 4M NaOH / dioxane / 1 h / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 2279-15-4
N-(benzyloxycarbonyl)-D-tryptophan

: 108827-21-0
N-α-benzyloxycarbonyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1.) HOBt, DCC; 2.) DIEA / dimethylformamide / 16 h / 4 °C

2: 99 percent / 4M NaOH / dioxane / 1 h / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;