(E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide

Base Information

• Chemical Name: (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide
• CAS No.: 1201799-09-8
• Molecular Formula: C₁₉H₁₆N₄O
• Molecular Weight: 316.362
• Mol file: 1201799-09-8.mol

Synonyms:(E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide

Chemical Property of (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide

There total 3 articles about (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C19H16N4O*ClH → (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide (1201799-09-8)

Guidance literature:

With sodium acetate; In ethanol; water; at 20 ℃; for 1h;

DOI:10.1107/S2053229618016467

Reference yield:

phenyl(pyridin-2-yl)methanone (91-02-1) → (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide (1201799-09-8)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 6 h / Reflux

2: sodium acetate / ethanol; water / 1 h / 20 °C

With sodium acetate; In ethanol; water;

DOI:10.1107/S2053229618016467

Reference yield:

4-phenylsemicarbazide hydrochloride (5441-14-5) → (E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide (1201799-09-8)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 6 h / Reflux

2: sodium acetate / ethanol; water / 1 h / 20 °C

With sodium acetate; In ethanol; water;

DOI:10.1107/S2053229618016467

upstream raw materials:

phenyl(pyridin-2-yl)methanone

4-phenylsemicarbazide hydrochloride

Downstream raw materials:

[copper(II)((E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide)(dichloride)]

[copper(II)((E)-N-phenyl-2-[phenyl(pyridine-2-yl)methylene]hydrazinecarboxamide)(dibromide)]