8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Base Information

Chemical Name:8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole
CAS No.:1050446-71-3
Molecular Formula:C₂₂H₂₆N₂
Molecular Weight:318.462
Hs Code.:

Synonyms:8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

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Chemical Property of 8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

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Technology Process of 8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

There total 5 articles about 8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1050446-68-8
[1-benzyl-3-(3-methylbut-2-enyl)-2-oxo-2,3-dihydro-1H-indol-3-yl]acetonitrile

: 1050446-71-3
8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Inert atmosphere; Cooling with ice; Reflux;

Reference yield:

: 60857-68-3
(1-benzyl-2-oxo-2,3-dihydro-1H-indol-3-yl)acetonitrile

: 1050446-71-3
8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

1.2: 0.5 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 5 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.2174/1386207318666150629114908

Reference yield:

: 59414-85-6
2-(1-benzyl-1H-indol-3-yl)acetonitrile

: 1050446-71-3
8-benzyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; acetic acid; water; dimethyl sulfoxide / 2 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

2.2: 0.5 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 5 °C / Inert atmosphere; Reflux

With hydrogenchloride; lithium aluminium tetrahydride; water; sodium hydride; acetic acid; dimethyl sulfoxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.2174/1386207318666150629114908