(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

Base Information

Chemical Name:(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione
CAS No.:1351534-11-6
Molecular Formula:C₃₀H₂₄ClNO₃
Molecular Weight:481.978
Hs Code.:

Synonyms:(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

Suppliers and Price of (5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

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Technology Process of (5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

There total 6 articles about (5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1263280-80-3
(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-oxazolidine-2,4-dione

: 76-83-5
trityl chloride

: 1351534-11-6
(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm201061j

Reference yield:

: 1351534-08-1
(2R)-2-(4-chloro-3-methylphenyl)propane-1,2-diol

: 1351534-11-6
(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 10 % platinum on carbon; sodium hydrogencarbonate / water / 18 h / 70 °C

2: diethyl ether

3: sodium ethanolate / ethanol / 95 °C

4: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With 10 % platinum on carbon; sodium ethanolate; sodium hydrogencarbonate; triethylamine; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/jm201061j

Reference yield:

: 1351534-09-2
(2R)-2-(4-chloro-3-methylphenyl)2-hydroxypropanoic acid

: 1351534-11-6
(5R)-5-(4-chloro-3-methylphenyl)-5-methyl-N-trityl-oxazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: sodium ethanolate / ethanol / 95 °C

3: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With sodium ethanolate; triethylamine; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm201061j