t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

Base Information

Chemical Name:t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate
CAS No.:864070-77-9
Molecular Formula:C₂₇H₂₈N₄O₉
Molecular Weight:552.541
Hs Code.:

Synonyms:t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

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Chemical Property of t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

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Technology Process of t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

There total 6 articles about t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 864070-76-8
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6-O-p-toluenesulfonyl-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

: 864070-77-9
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

Guidance literature:: With sodium azide; 15-crown-5; In N,N-dimethyl-formamide; for 24h;
DOI:10.1016/j.tet.2005.06.022

Reference yield:

: 544703-54-0
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-β-D-galactopyranosyl-oxy)-3-p-hydroxyphenyl-2-acrylate

: 864070-77-9
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

Guidance literature:: With sodium azide; 15-crown-5; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2003.10.150

Reference yield:

: 864070-74-6
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-β-D-galactopyranosyloxy)-3-p-t-butyldimethylsilyloxyphenyl-2-acrylate

: 864070-77-9
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-p-hydroxyphenyl-2-acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / pyridine / 25 h

2: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C

3: 100 percent / sodium azide; 15-crown-5 / dimethylformamide / 24 h

With pyridine; sodium azide; 15-crown-5; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.022