Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat

Base Information

Chemical Name:Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat
CAS No.:147919-03-7
Molecular Formula:C₃₄H₂₈O₁₂
Molecular Weight:628.589
Hs Code.:

Synonyms:Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat

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Chemical Property of Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat

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Technology Process of Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat

There total 2 articles about Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 147919-00-4
2,6-Bis-(2-acetyl-4-methoxycarbonylphenyl)-1,5-dimethoxynaphthalindicarboxylat

: 147919-03-7
Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; acetone; for 8h; Heating;
DOI:10.1002/ardp.19933260310

Reference yield:

: 57009-12-8
methyl 3-acetyl-4-hydroxybenzoate

: 147919-03-7
Dimethyl-2',6'-bis-<2-(2-hydroxybenzoyl)-1-hydroxyvinylen>-1',5'-dimethoxynaphthalin-5,5-dicarboxylat

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / K₂CO₃ / acetone / 10 h / Ambient temperature

2: 56 percent / K₂CO₃ / acetone; dimethylformamide / 8 h / Heating

With potassium carbonate; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/ardp.19933260310