N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide

Base Information

• Chemical Name: N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide
• CAS No.: 934271-06-4
• Molecular Formula: C₄₂H₆₀N₂O₅Si
• Molecular Weight: 701.034
• Mol file: 934271-06-4.mol

Synonyms:N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide

Chemical Property of N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide

There total 1 articles about N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C43H61ClN4O8SSi (934271-05-3) → N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide (934271-06-4)

Guidance literature:

With sodium iodide; In dimethyl sulfoxide; at 20 ℃; for 48h;

DOI:10.1016/j.tetasy.2008.03.018

Reference yield:

N,N-diethyl-2,6-dideoxy-2,6-imino-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-L-glycero-D-allo-heptonamide (934271-06-4) + acetic anhydride (108-24-7) → C44H62N2O6Si (934271-07-5)

Guidance literature:

With pyridine; for 144h;

DOI:10.1016/j.tetasy.2008.03.018

upstream raw materials:

C₄₃H₆₁ClN₄O₈SSi

Downstream raw materials:

C₄₄H₆₂N₂O₆Si