5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Base Information

Chemical Name:5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid
CAS No.:128950-05-0
Molecular Formula:C₂₈H₃₀O₇S
Molecular Weight:510.608
Hs Code.:

Synonyms:5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

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Chemical Property of 5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Chemical Property:

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Technology Process of 5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

There total 7 articles about 5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-[3-(2-Ethoxycarbonyl-ethyl)-4-(6-phenyl-hexyloxy)-benzenesulfonyl]-benzoic acid ethyl ester

: 128950-05-0
5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Guidance literature:: With potassium hydroxide; In methanol; water; at 25 ℃; for 4h; Yield given;
DOI:10.1021/jm00172a019

Reference yield:

: 128950-13-0
4-<(3-carboxyphenyl)thio>phenol

: 128950-05-0
5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / sulfuric acid / 96 h / Heating

2: 100 percent / pivalic acid / toluene / Heating

3: 86 percent / 1 N HCl, ethanol / 0.5 h / 25 °C

4: 1.) NaH / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C, overnight

5: m-chloroperoxybenzoic acid (mPCBA) / CH₂Cl₂ / 2 h / 0 °C

6: KOH / methanol; H₂O / 4 h / 25 °C

With hydrogenchloride; potassium hydroxide; ethanol; sulfuric acid; sodium hydride; 3-chloro-benzenecarboperoxoic acid; Trimethylacetic acid; In methanol; dichloromethane; water; toluene;
DOI:10.1021/jm00172a019

Reference yield:

: 128950-14-1
4-<(3-carboxyphenyl)thio>anisole

: 128950-05-0
5-<(3-carboxyphenyl)sulfonyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / pyridine hydrochloride / 4 h / 180 °C

2: 68 percent / sulfuric acid / 96 h / Heating

3: 100 percent / pivalic acid / toluene / Heating

4: 86 percent / 1 N HCl, ethanol / 0.5 h / 25 °C

5: 1.) NaH / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C, overnight

6: m-chloroperoxybenzoic acid (mPCBA) / CH₂Cl₂ / 2 h / 0 °C

7: KOH / methanol; H₂O / 4 h / 25 °C

With hydrogenchloride; potassium hydroxide; ethanol; sulfuric acid; pyridine hydrochloride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; Trimethylacetic acid; In methanol; dichloromethane; water; toluene;
DOI:10.1021/jm00172a019